Chapter NR 660

NR 660.10 Note Note: See chs. 289 and 291, Stats., for additional definitions.

NR 660.10 History History: CR 05-032: cr. Register July 2006 No. 607, eff. 8-1-06; CR 06-102: am. (21), (76) and (77) Register March 2007 No. 615, eff. 4-1-07; EmR1007: emerg. cr. (70m), am. (107), eff. 3-17-10; CR 10-036: cr. (70m), am. (107) Register October 2010 No. 658, eff. 11-1-10; corrections in (15), (141) made under s. 13.92 (4) (b) 7., Stats., Register March 2013 No. 687; CR 16-007: cr. (9m), (19d), (19g), (19j), am. (43) (b), (70m) (a) to (c), cr. (77m), (83m), am. (107) (a), (b), cr. (108m), am. (133) (c), renum. (139) to (139) (intro.) and (a), cr. (139) (b), (c), (145m) Register July 2017 No. 739, eff. 8-1-17; correction in (9m), (43) (b), (83m), (108m) (b) made under s. 35.17, Stats., and correction in numbering of (108m) made under s. 13.92 (4) (b) 1., Stats., Register July 2017 No. 739; CR 19-082: cr. (3m), (3p), (3t), (3w), (3y), (9t), (13m), (19e), (20m), r. and recr. (21), cr. (28m), (28p), (28s), am (29) (a), (31), (34), (43) (a), (b), (46), cr. (50m), (51m), (51t), am. (52), (53), cr. (65m), (67m), r. and recr. (70m), am. (76), (82), (83m), cr. (83t), (97m), (97t), (100m), r. and recr. (107), am. (108), (108m) (a) 1., 3., (b), (122), (126) (b), cr. (138m), r. and recr. (139), am. (141) (b) Register August 2020 No. 776, eff. 9-1-20; correction in (13m) (c), (d), (28), (38), (51m), (60) (g), (82), (83m), (108m) (b), (126) (b) made under s. 35.17, Stats., Register August 2020 No. 776; correction in (50m) made under s. 13.92 (4) (b) 7., Stats., Register April 2021 No. 784; CR 24-036: cr. (3o), am. (133) (c), cr. (133) (e), am. (134) (b) 1. Register May 2025 No. 833, eff. 6-1-25; correction in (50m) made under s. 35.17, Stats., Register May 2025 No. 833.

NR 660.11 NR 660.11 Incorporation by reference.

NR 660.11(1) (1) This section is adopted under ss. 227.21 (2) (b) and 291.05, Stats., to incorporate by reference testing, monitoring, and other technical standards, established by the federal government and technical societies and organizations, to which reference is made under chs. NR 660 to 679. Materials that are incorporated by reference in other references are hereby incorporated by reference and made a part of this subsection.

NR 660.11 Note Note: Copies of these materials are available for inspection in the office of the Legislative Reference Bureau or may be obtained for personal use at the addresses noted.

NR 660.11(2) (2) The following materials are available for purchase from the American Society for Testing and Materials, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428–2959, [phone], www.astm.org:

NR 660.11(2)(a) (a) ASTM D93–79, Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021.

NR 660.11(2)(b) (b) ASTM D93–80, Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021.

NR 660.11(2)(c) (c) ASTM D1946–82, Standard Method for Analysis of Reformed Gas by Gas Chromatography, incorporated by reference for ss. NR 664.1033 and 665.1033.

NR 660.11(2)(d) (d) ASTM D2267–88, Standard Test Method for Aromatics in Light Naphthas and Aviation Gasolines by Gas Chromatography, incorporated by reference for s. NR 664.1063.

NR 660.11(2)(e) (e) ASTM D2382–83, Standard Test Method for Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method), incorporated by reference for ss. NR 664.1033 and 665.1033.

NR 660.11(2)(f) (f) ASTM D2879–92, Standard Test Method for Vapor Pressure—Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope, incorporated by reference for s. NR 665.1084.

NR 660.11(2)(g) (g) ASTM D3278–78, Standard Test Methods for Flash Point for Liquids by Setaflash Closed Tester, incorporated by reference for s. NR 661.0021 (1).

NR 660.11(2)(h) (h) ASTM D8174-18, Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small Scale Closed Cup Tester, incorporated by reference for s. NR 661.0021 (1).

NR 660.11(2)(i) (i) ASTM D8175-18, Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021 (1).

NR 660.11(2)(j) (j) ASTM E168–88, Standard Practices for General Techniques of Infrared Quantitative Analysis, incorporated by reference for s. NR 664.1063.

NR 660.11(2)(k) (k) ASTM E169–87, Standard Practices for General Techniques of Ultraviolet-Visible Quantitative Analysis, incorporated by reference for s. NR 664.1063.

NR 660.11(2)(L) (L) ASTM E260–85, Standard Practice for Packed Column Gas Chromatography, incorporated by reference for s. NR 664.1063.

NR 660.11(2)(m) (m) ASTM E681-09, Standard Test Method for Concentration Limits of Flammability of Chemicals (Vapors and Gases), incorporated by reference for s. NR 661.0021 (1).

NR 660.11(2)(n) (n) ASTM D323-20, Standard Test Method for Vapor Pressure of Petroleum Products (Reid Method), incorporated by reference for s. NR 661.0021 (1).

NR 660.11(2)(o) (o) ASTM D140-70, Standard Practice for Sampling Bituminous Materials, incorporated by reference for ch. NR 661 Appendix I.

NR 660.11(2)(p) (p) ASTM D346-75, Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis, incorporated by reference for ch. NR 661 Appendix I.

NR 660.11(2)(q) (q) ASTM D420-69, Guide to Site Characterization for Engineering, Design, and Construction Purposes, incorporated by reference for ch. NR 661 Appendix I.

NR 660.11(2)(r) (r) ASTM D1452-65, Standard Practice for Soil Investigation and Sampling by Auger Borings, incorporated by reference for ch. NR 661 Appendix I.

NR 660.11(2)(s) (s) ASTM D2234-76, Standard Practice for Collection of a Gross Sample of Coal, incorporated by reference for ch. NR 661 Appendix I.

NR 660.11(2)(t) (t) ASTM D2879-86, Standard Test Method for Vapor Pressure—Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope, incorporated by reference for ch. NR 664 and subch. BB of ch. NR 665.

NR 660.11(2)(u) (u) ASTM G21-70 (1984a), Standard Practice for Determining Resistance of Synthetic Polymer Materials to Fungi, incorporated by reference for ch. NR 664 and subch. N of ch. NR 665.

NR 660.11(2)(v) (v) ASTM G22-76 (1984b), Standard Practice for Determining Resistance of Plastics to Bacteria, incorporated by reference for ch. NR 664 and subch. N of ch. NR 665.

NR 660.11(3) (3) The following materials are available for purchase from the National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22161; or for purchase from the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402, (202) 512–1800:

NR 660.11(3)(a) (a) APTI Course 415: Control of Gaseous Emissions, EPA Publication EPA–450/2–81– 005, December 1981, incorporated by reference for ss. NR 661.1035, 664.1035, 665.1035, 670.024, and 670.025.

NR 660.11(3)(b) (b) Screening Procedures for Estimating the Air Quality Impact of Stationary Sources, Revised, October 1992, EPA Publication EPA–450/R–92–019, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(3)(c) (c) The following methods as published in the test methods compendium known as “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846, Third Edition:

NR 660.11(3)(c)1. 1. Method 0011, Revision 1, August 2018, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(3)(c)2. 2. Method 0023A, Revision 2, August 2018, incorporated by reference for s. NR 666.104 and ch. NR 666 Appendix IX.

NR 660.11(3)(c)3. 3. Method 0050, December 1996, and Update III, incorporated by reference for s. NR 666.107 and ch. NR 666 Appendix IX.

NR 660.11(3)(c)4. 4. Method 0051, Revision 1, August 2018, incorporated by reference for s. NR 666.107 and ch. NR 666 Appendix IX.

NR 660.11(3)(c)5. 5. Method 0060, December 1996, and Update III, incorporated by reference for s. NR 666.106 and ch. NR 666 Appendix IX.

NR 660.11(3)(c)6. 6. Method 0061, December 1996 and Update III, incorporated by reference for s. NR 666.106 and ch. NR 666 Appendix IX.

NR 660.11(3)(c)7. 7. Method 1010B, December 2018, incorporated by reference for s. NR 661.0021.

NR 660.11(3)(c)8. 8. Method 1020C, December 2018, incorporated by reference for s. NR 661.0021.

NR 660.11(3)(c)9. 9. Method 1110A, November 2004 and Update IIIB, incorporated by reference for s. NR 661.0022.

NR 660.11(3)(c)10. 10. Method 1311, July 1992, and Update I, incorporated by reference for ss. NR 661.0024, 664.0552, 668.07, 668.40, and ch. NR 661 Appendix IX.

NR 660.11(3)(c)11. 11. Method 1330A, Extraction Procedure for Oily Wastes, dated July 1992 and in Update I, incorporated by reference for ch. NR 661 Appendix IX.

NR 660.11(3)(c)12. 12. Method 9010C, dated November 2004 and Update IIIB, incorporated by reference for ss. NR 668.40, 668.44, and 668.48.

NR 660.11(3)(c)13. 13. Method 9012B, November 2004 and Update IIIB, incorporated by reference for ss. NR 668.40, 668.44, and 668.48.

NR 660.11(3)(c)14. 14. Method 9040C, November 2004 and Update IIIB, incorporated by reference for s. NR 661.0022.

NR 660.11(3)(c)15. 15. Method 9060A, November 2004 and Update IIIB, incorporated by reference for ss. NR 664.1034, 664.1063, 665.1034, and 665.1063

NR 660.11(3)(c)16. 16. Method 9071B, n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples, dated April 1998 and in Update IIIA, incorporated by reference for ch. NR 661 Appendix IX.

NR 660.11(3)(c)17. 17. Method 9095B, November 2004 and Update IIIB, incorporated by reference for ss. NR 664.0190, 664.0314, 665.0190, 665.0314, 665.1081, 667.0190 (1), and 668.32.

Note: A suffix of “A” in the method number indicates revision one (the method has been revised once). A suffix of “B” in the method number indicates revision two (the method has been revised twice). A suffix of “C” in the method number indicates revision three (the method has been revised three times). A suffix of “D” in the method number indicates revision four (the method has been revised four times).

NR 660.11(4) (4) The following materials are available for purchase from the National Fire Protection Association, 1 Batterymarch Park, P.O. Box 9101, Quincy, MA 02269–9101, [phone], www.nfpa.org:

NR 660.11(4)(a) (a) Flammable and Combustible Liquids Code (NFPA 30), (1977), incorporated by reference for ss. NR 662.016 (2), 664.0198, and 665.0198, subch. H of ch. NR 666, and s. NR 667.0202 (2).

NR 660.11(4)(b) (b) Flammable and Combustible Liquids Code (NFPA 30), (1981), incorporated by reference for ss. NR 662.016 (2), 664.0198, and 665.0198, subch. H of ch. NR 666, and s. NR 667.0202 (2).

NR 660.11(5) (5) The following materials are available for purchase from the Organization for Economic Co-operation and Development, Environment Directorate, 2 rue André Pascal, F-75775 Paris Cedex 16, France, www.oecd-ilibrary.org:

NR 660.11(5)(a) (a) Guidance Manual for the Control of Transboundary Movements of Recoverable Wastes, copyright 2009, Annex B: OECD Consolidated List of Wastes Subject to the Green Control Procedure and Annex C: OECD Consolidated List of Wastes Subject to the Amber Control Procedure, incorporated by reference for ss. NR 662.082 (1), 662.083 (2), (4), and (7), and 662.084 (2) and (4).

NR 660.11(6) (6) The following materials are available for purchase from the American Petroleum Institute, 1220 L Street, Northwest, Washington, DC 20005:

NR 660.11(6)(a) (a) American Petroleum Institute Publication 2517, Third Edition, February 1989, Evaporative Loss from External Floating-Roof Tanks, incorporated by reference for s. NR 665.1084.

NR 660.11(6)(b) (b) American Petroleum Institute Publication, Guide for Inspection of Refinery Equipment, Chapter XIII, “Atmospheric and Low-Pressure Storage Tanks,” 4th edition, 1981, incorporated by reference for s. NR 661.0191 (2).

NR 660.11(7) (7) The following materials are available for purchase from the Steel Tank Institute, 944 Donata Court, Lake Zurich, IL 60047:

NR 660.11(7)(a) (a) Steel Tank Institute, “Standard for Dual Wall Underground Storage Tanks,” 2006, incorporated by reference for s. NR 661.0193 (4).

NR 660.11(8) (8) The following Code of Federal Regulation Appendices are available for purchase from Superintendent of Documents, PO Box 371954, Pittsburgh, PA 15250-7954, [phone]:

NR 660.11(8)(a) (a) 40 CFR part 51, Appendix M, Method 204 Criteria for and Verification of a Permanent or Temporary Total Enclosure incorporated by reference for subch. CC of ch. NR 664 and subch. CC of ch. NR 665.

NR 660.11(8)(b) (b) 40 CFR part 51, Appendix W Guideline on Air Quality Models (Revised), incorporated by reference for subch. H of ch. NR 666.

NR 660.11(8)(c) (c) 40 CFR part 60, Appendix A Test Methods, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(8)(d) (d) 40 CFR part 60, Appendix A, Methods 1 to 5 Various Titles, incorporated by reference for subch. H of ch. NR 666.

NR 660.11(8)(e) (e) 40 CFR part 60, Appendix A, Method 1 Sample and Velocity Traverses for Stationary Sources, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(8)(f) (f) 40 CFR part 60, Appendix A, Method 2 Determination of Stack Gas Velocity and volumetric Flow Rate (Type S Pitot Tube) incorporated by reference for subch. AA of ch. NR 664 and subch. AA of ch. NR 665.

NR 660.11(8)(g) (g) 40 CFR part 60, Appendix A, Method 2A Direct Measurement of Gas Volume through Pipes and Small Ducts, incorporated by reference for subch. AA of ch. NR 664 and subch. AA of ch. NR 665.

NR 660.11(8)(h) (h) 40 CFR part 60, Appendix A, Method 2C Determination of Gas Velocity and Volumetric Flow Rate in Small Stacks or Ducts (Standard Pitot Tube) incorporated by reference for subch. AA of ch. NR 664 and subch. AA of ch. NR 665.

NR 660.11(8)(i) (i) 40 CFR part 60, Appendix A, Method 2D Measurement of Gas Volume Flow Rates in Small Pipes and Ducts, incorporated by reference for subch. AA of ch. NR 664 and subch. AA of ch. NR 665.

NR 660.11(8)(j) (j) 40 CFR part 60, Appendix A, Method 3 Gas Analysis for the Determination of Dry Molecular Weight, incorporated by reference for subch. O of ch. NR 664 and ch. NR 666 Appendix IX.

NR 660.11(8)(k) (k) 40 CFR part 60, Appendix A, Method 3A, Determination of Oxygen and Carbon Dioxide Concentrations in Emissions from Stationary Sources (Instrumental Analyzer Procedure), incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(8)(L) (L) 40 CFR part 60, Appendix A, Method 10 Determination of Carbon Monoxide Emissions from Stationary Sources, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(8)(m) (m) 40 CFR part 60, Appendix A, Method 10A Determination of Carbon Monoxide Emissions in Certifying Continuous Emission Monitoring Systems at Petroleum Refineries, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(8)(n) (n) 40 CFR part 60, Appendix A, Method 10B Determination of Carbon Monoxide Emissions from Stationary Sources, incorporated by reference for ch. NR 666 Appendix IX.

NR 660.11(8)(o) (o) 40 CFR part 60, Appendix A, Method 18 Measurement of Gaseous Organic Compound Emissions by Gas Chromatography, incorporated by reference for subch. AA of ch. NR 664 and subch. AA of ch. NR 665.

NR 660.11(8)(p) (p) 40 CFR part 60, Appendix A, Method 21 Determination of Volatile Organic Compounds Leaks, incorporated by reference for subchs. AA, BB, and CC of ch. NR 664 and subchs. AA, BB, and CC of ch. NR 665.

NR 660.11(8)(q) (q) 40 CFR part 60, Appendix A, Method 22 Visual Determination of Fugitive Emissions from Material Sources and Smoke Emissions from Flares, incorporated by reference for subchs. AA and DD of ch. NR 664 and subchs. AA and DD of ch. NR 665.

NR 660.11(8)(r) (r) 40 CFR part 60, Appendix A, Method 25D Determination of the Volatile Organic Concentration of Waste Samples, incorporated by reference for subch. CC of ch. NR 664 and subch. CC of ch. NR 665.

NR 660.11(8)(s) (s) 40 CFR part 60, Appendix A, Method 25E Determination of Vapor Phase Organic concentration in Waste Samples, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(t) (t) 40 CFR part 60, Appendix A, Method 27 Determination of Vapor Tightness of Gasoline Delivery Tank using Pressure-Vacuum Test, incorporated by reference for subch. CC of ch. NR 664.

NR 660.11(8)(u) (u) 40 CFR part 63, Appendix A, Method 301 Field Validation of Pollutant Measurement Methods from Various Waste Media, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(v) (v) 40 CFR part 63, Appendix C Determination of the Fraction Biodegraded (Fbio) in a Biological Treatment Unit, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(w) (w) 40 CFR part 63, Appendix D Alternative Validation Procedure for EPA Waste and Wastewater Methods, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(x) (x) 40 CFR part 136, Appendix A, Method 624 Purgeables, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(y) (y) 40 CFR part 136, Appendix A, Method 625 Base/Neutrals and Acids, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(z) (z) 40 CFR part 136, Appendix A, Method 1624 Volatile Organic Compounds by Isotope Dilution GC/MS, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(za) (za) 40 CFR part 136, Appendix A, Method 1625 Semivolatile Organic Compounds by Isotope Dilution GC/MS, incorporated by reference for subch. CC of ch. NR 665.

NR 660.11(8)(zb) (zb) 40 CFR 52.741, Appendix B, Method 204 Procedure T—Criteria for and Verification of a Permanent or Temporary Total Enclosure, incorporated by reference for ss. NR 661.1084 (9), 661.1086 (5), 661.1089 (2), 661.1089 (4), 670.027 (1), and 670.315 (3).